An updated set of hands-on labs were released for C# and VB.NET enterprise developers, including exercises for application blocks, Unity, interception and complex configuration scenarios.
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The set contains a guide to learn about the application blocks included with Microsoft Enterprise Library 5.0 and practice how to leverage their capabilities in various application contexts. It includes Caching, Configuration Sources, Cryptography, Data Access, Exception Handling, Interception, Logging, Security, Validation, and Unity Hands-on Labs.
You can download the hands-on lab using this link, however to download Enterprise Library 5.0 please use this link.
An Introduction to Enterprise Library 5.0
Microsoft Enterprise Library is a collection of reusable application blocks designed to assist software developers with common enterprise development challenges. 
